or loss of muscle control (l.m.c.) General Methods for Preparation of the Allyl Ethers (4) These compounds were prepared by ... (a) 4-Chloro-6, 6-dimethyl-2, 5, 6 , 7-tetrahydro-l#-azepin-2-one (2 0g, 11 -5 mmol) was added to a solution of sodium (0-24 g) in the ... Elution with dichloromethane/ethanol (19 : 1) gave the ether (72%), m.p. 83-84-5Ad, after recrystallization from light ... N.m.r.: alt;5 7-3, br, NH; 5-60, m, CH-CH; 4 92, s, OC=CH; 4-24, d, J 6 Hz, OCH2; 2-87, d, 7 6 Hz, CH2N; 2- 17, s, anbsp;...
Title | : | Australian Journal of Chemistry |
Author | : | |
Publisher | : | - 1980 |
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